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2020 Journal Article Organophotocatalytic N‐demethylation of oxycodone using molecular oxygenChen, Yuesu, Glotz, Gabriel, Cantillo, David and Kappe, C. Oliver (2020). Organophotocatalytic N‐demethylation of oxycodone using molecular oxygen. Chemistry: A European Journal, 26 (13), 2973-2979. doi: 10.1002/chem.201905505 |
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2020 Journal Article Translating batch electrochemistry to single-pass continuous flow conditions: an organic chemist’s guideMaljuric, Snjezana, Jud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2020). Translating batch electrochemistry to single-pass continuous flow conditions: an organic chemist’s guide. Journal of Flow Chemistry, 10 (1), 181-190. doi: 10.1007/s41981-019-00050-z |
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2019 Journal Article Continuous flow synthesis of terminal epoxides from ketones using in situ generated bromomethyl lithiumvon Keutz, Timo, Cantillo, David and Kappe, C. Oliver (2019). Continuous flow synthesis of terminal epoxides from ketones using in situ generated bromomethyl lithium. Organic Letters, 21 (24), 10094-10098. doi: 10.1021/acs.orglett.9b04072 |
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2019 Journal Article Continuous flow synthesis of methyl oximino acetoacetate: accessing greener purification methods with inline liquid–liquid extraction and membrane separation technologyLebl, René, Murray, Trevor, Adamo, Andrea, Cantillo, David and Kappe, C. Oliver (2019). Continuous flow synthesis of methyl oximino acetoacetate: accessing greener purification methods with inline liquid–liquid extraction and membrane separation technology. ACS Sustainable Chemistry and Engineering, 7 (24), 20088-20096. doi: 10.1021/acssuschemeng.9b05954 |
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2019 Journal Article Cathodic C–H trifluoromethylation of arenes and heteroarenes enabled by an in situ-generated triflyltriethylammonium complexJud, Wolfgang, Maljuric, Snjezana, Kappe, C. Oliver and Cantillo, David (2019). Cathodic C–H trifluoromethylation of arenes and heteroarenes enabled by an in situ-generated triflyltriethylammonium complex. Organic Letters, 21 (19), 7970-7975. doi: 10.1021/acs.orglett.9b02948 |
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2019 Journal Article Continuous generation, in-line quantification and utilization of nitrosyl chloride in photonitrosation reactionsLebl, Rene, Cantillo, David and Kappe, C. Oliver (2019). Continuous generation, in-line quantification and utilization of nitrosyl chloride in photonitrosation reactions. Reaction Chemistry and Engineering, 4 (4), 738-746. doi: 10.1039/c8re00323h |
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2019 Journal Article Visible light‐promoted Beckmann rearrangements: separating sequential photochemical and thermal phenomena in a continuous flow reactorChen, Yuesu, Cantillo, David and Kappe, C. Oliver (2019). Visible light‐promoted Beckmann rearrangements: separating sequential photochemical and thermal phenomena in a continuous flow reactor. European Journal of Organic Chemistry, 2019 (11), 2163-2171. doi: 10.1002/ejoc.201900231 |
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2019 Journal Article Enhanced mixing of biphasic liquid-liquid systems for the synthesis of gem-dihalocyclopropanes using packed bed reactorsvon Keutz, Timo, Cantillo, David and Kappe, C. Oliver (2019). Enhanced mixing of biphasic liquid-liquid systems for the synthesis of gem-dihalocyclopropanes using packed bed reactors. Journal of Flow Chemistry, 9 (1), 27-34. doi: 10.1007/s41981-018-0026-1 |
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2019 Journal Article Continuous-flow protocol for the synthesis of enantiomerically pure intermediates of anti epilepsy and anti tuberculosis active pharmaceutical ingredientsAguiar, Renata M., Leão, Raquel A. C., Mata, Alejandro, Cantillo, David, Kappe, C. Oliver, Miranda, Leandro S. M. and de Souza, Rodrigo O. M. A. (2019). Continuous-flow protocol for the synthesis of enantiomerically pure intermediates of anti epilepsy and anti tuberculosis active pharmaceutical ingredients. Organic and Biomolecular Chemistry, 17 (6), 1552-1557. doi: 10.1039/c8ob03088j |
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2019 Journal Article On the reactivity of anodically generated trifluoromethyl radicals toward aryl alkynes in organic/aqueous mediaJud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2019). On the reactivity of anodically generated trifluoromethyl radicals toward aryl alkynes in organic/aqueous media. Organic and Biomolecular Chemistry, 17 (14), 3529-3537. doi: 10.1039/c9ob00456d |
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2018 Journal Article Catalyst‐free oxytrifluoromethylation of alkenes through paired electrolysis in organic‐aqueous mediaJud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2018). Catalyst‐free oxytrifluoromethylation of alkenes through paired electrolysis in organic‐aqueous media. Chemistry: A European Journal, 24 (65), 17234-17238. doi: 10.1002/chem.201804708 |
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2018 Journal Article Continuous flow photochemical benzylic bromination of a key intermediate in the synthesis of a 2-oxazolidinoneChen, Yuesu, de Frutos, Oscar, Mateos, Carlos, Rincon, Juan A., Cantillo, David and Kappe, C. Oliver (2018). Continuous flow photochemical benzylic bromination of a key intermediate in the synthesis of a 2-oxazolidinone. Chemphotochem, 2 (10), 906-912. doi: 10.1002/cptc.201800114 |
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2018 Journal Article Continuous flow multistep synthesis of α-functionalized esters via lithium enolate intermediatesvon Keutz, Timo, Strauss, Franz J., Cantillo, David and Kappe, C. Oliver (2018). Continuous flow multistep synthesis of α-functionalized esters via lithium enolate intermediates. Tetrahedron, 74 (25), 3113-3117. doi: 10.1016/j.tet.2017.11.063 |
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2018 Journal Article Review of Timothy Noël (ed): photochemical processes in continuous flow reactors: from engineering principles to chemical applicationsCantillo, David (2018). Review of Timothy Noël (ed): photochemical processes in continuous flow reactors: from engineering principles to chemical applications. Journal of Flow Chemistry, 8 (2), 107-108. doi: 10.1007/s41981-018-0011-8 |
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2018 Journal Article Process intensification and integration studies for the generation of a key aminoimidazole intermediate in the synthesis of lanabecestatZnidar, Desiree, Cantillo, David, Inglesby, Phillip, Boyd, Alistair and Kappe, C. Oliver (2018). Process intensification and integration studies for the generation of a key aminoimidazole intermediate in the synthesis of lanabecestat. Organic Process Research and Development, 22 (5), 633-640. doi: 10.1021/acs.oprd.8b00089 |
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2018 Journal Article Continuous multistep synthesis of 2-(azidomethyl)oxazolesRossa, Thais A., Suveges, Nicolas S., Sa, Marcus M., Cantillo, David and Kappe, C. Oliver (2018). Continuous multistep synthesis of 2-(azidomethyl)oxazoles. Beilstein Journal of Organic Chemistry, 14, 506-514. doi: 10.3762/bjoc.14.36 |
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2017 Journal Article Hydrogen sulfide chemistry in continuous flow: Efficient synthesis of 2-oxopropanethioamideCantillo, David, Inglesby, Phillip A., Boyd, Alistair and Kappe, C. Oliver (2017). Hydrogen sulfide chemistry in continuous flow: Efficient synthesis of 2-oxopropanethioamide. Journal of Flow Chemistry, 7 (2), 29-32. doi: 10.1556/1846.2017.00006 |
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2017 Journal Article An integrated continuous-flow synthesis of a key oxazolidine intermediate to noroxymorphone from naturally occurring opioidsMata, Alejandro, Cantillo, David and Kappe, C. Oliver (2017). An integrated continuous-flow synthesis of a key oxazolidine intermediate to noroxymorphone from naturally occurring opioids. European Journal of Organic Chemistry, 2017 (44), 6505-6510. doi: 10.1002/ejoc.201700811 |
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2017 Journal Article Halogenation of organic compounds using continuous flow and microreactor technologyCantillo, David and Kappe, C. Oliver (2017). Halogenation of organic compounds using continuous flow and microreactor technology. Reaction Chemistry and Engineering, 2 (1), 7-19. doi: 10.1039/c6re00186f |
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2017 Journal Article Design and development of Pd-catalyzed aerobic N-demethylation strategies for the synthesis of noroxymorphone in continuous flow modeGutmann, Bernhard, Cantillo, David, Weigl, Ulrich, Cox, D. Phillip and Kappe, C. Oliver (2017). Design and development of Pd-catalyzed aerobic N-demethylation strategies for the synthesis of noroxymorphone in continuous flow mode. European Journal of Organic Chemistry, 2017 (4), 914-927. doi: 10.1002/ejoc.201601453 |
