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2024 Journal Article Merging Inline NMR Monitoring and Flow Chemistry in the Undergraduate Organic Chemistry LaboratoryWelch, Bradley Graeme and Cantillo, David (2024). Merging Inline NMR Monitoring and Flow Chemistry in the Undergraduate Organic Chemistry Laboratory. Journal of Chemical Education, 101 (8), 3459-3465. doi: 10.1021/acs.jchemed.4c00429 |
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2024 Journal Article Design of Experiments-Based Optimization of an Electrochemical Decarboxylative Alkylation Using a Spinning Cylinder Electrode ReactorPetrović, Nikola, Cumming, Graham R., Hone, Christopher A., Nieves-Remacha, María José, García-Losada, Pablo, de Frutos, Óscar, Kappe, C. Oliver and Cantillo, David (2024). Design of Experiments-Based Optimization of an Electrochemical Decarboxylative Alkylation Using a Spinning Cylinder Electrode Reactor. Organic Process Research & Development, 28 (7), 2928-2934. doi: 10.1021/acs.oprd.4c00178 |
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2024 Journal Article Recent advances in synthetic organic electrochemistry using flow systemsCantillo, David (2024). Recent advances in synthetic organic electrochemistry using flow systems. Current Opinion in Electrochemistry, 44 101459, 101459. doi: 10.1016/j.coelec.2024.101459 |
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2024 Journal Article Scalable Quasi-Divided Cell Operation Using Spinning Cylinder Electrode Technology: Multigram Electrochemical Synthesis of an Axitinib IntermediateMalviya, Bhanwar K., Hansen, Eric C., Kong, Caleb J., Imbrogno, Joseph, Verghese, Jenson, Guinness, Steven M., Salazar, Chase A., Desrosiers, Jean-Nicolas, Kappe, C. Oliver and Cantillo, David (2024). Scalable Quasi-Divided Cell Operation Using Spinning Cylinder Electrode Technology: Multigram Electrochemical Synthesis of an Axitinib Intermediate. Organic Process Research & Development, 28 (3), 790-797. doi: 10.1021/acs.oprd.3c00508 |
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2024 Journal Article Aniline derivatives from lignin under mild conditions enabled by electrochemistryCastillo-Garcia, Antonio A., Kappe, Christian Oliver, Cantillo, David and Barta, Katalin (2024). Aniline derivatives from lignin under mild conditions enabled by electrochemistry. ChemSusChem, 17 (3) e202301374. doi: 10.1002/cssc.202301374 |
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2024 Journal Article Electrochemical synthesis: A flourishing green technology for the manufacturing of organic compoundsCantillo, David (2024). Electrochemical synthesis: A flourishing green technology for the manufacturing of organic compounds. Current Research in Green and Sustainable Chemistry 100416, 100416. doi: 10.1016/j.crgsc.2024.100416 |
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2024 Journal Article Scalable catalyst free electrochemical chlorination of aminophenol derivatives enabled by a quasi-divided cell approachMalviya, Bhanwar K., Laudadio, Gabriele, Kappe, C. Oliver and Cantillo, David (2024). Scalable catalyst free electrochemical chlorination of aminophenol derivatives enabled by a quasi-divided cell approach. Green Chemistry. doi: 10.1039/d4gc03569k |
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2024 Journal Article Development of an open-source flow-through cyclic voltammetry cell for real-time inline reaction analyticsRial-Rodríguez, Eduardo, Williams, Jason D., Eggenweiler, Hans-Michael, Fuchss, Thomas, Sommer, Alena, Kappe, C. Oliver and Cantillo, David (2024). Development of an open-source flow-through cyclic voltammetry cell for real-time inline reaction analytics. Reaction Chemistry and Engineering, 9 (1), 26-30. doi: 10.1039/d3re00535f |
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2023 Journal Article Electrifying Friedel-Crafts intramolecular alkylation toward 1,1-disubstituted tetrahydronaphthalenesLunghi, Enrico, Ronco, Pietro, Della Negra, Federico, Trucchi, Beatrice, Verzini, Massimo, Merli, Daniele, Casali, Emanuele, Kappe, C Oliver, Cantillo, David and Zanoni, Giuseppe (2023). Electrifying Friedel-Crafts intramolecular alkylation toward 1,1-disubstituted tetrahydronaphthalenes. The Journal of Organic Chemistry, 88 (24), 16783-16789. doi: 10.1021/acs.joc.3c01281 |
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2023 Journal Article A Low-Volume Flow Electrochemical Microreactor for Rapid and Automated Process OptimizationRial-Rodríguez, Eduardo, Wagner, Johannes F., Eggenweiler, Hans-Michael, Fuchss, Thomas, Sommer, Alena, Kappe, C. Oliver, Williams, Jason and Cantillo, David (2023). A Low-Volume Flow Electrochemical Microreactor for Rapid and Automated Process Optimization. Reaction Chemistry & Engineering, 9 (1), 1-6. doi: 10.1039/d3re00586k |
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2023 Journal Article Multigram electrochemical Hofmann rearrangement using a spinning three-dimensional anodeMalviya, Bhanwar K., Bottecchia, Cecilia, Stone, Kevin, Lehnherr, Dan, Lévesque, François, Kappe, C. Oliver and Cantillo, David (2023). Multigram electrochemical Hofmann rearrangement using a spinning three-dimensional anode. Organic Process Research and Development, 27 (11), 2183-2191. doi: 10.1021/acs.oprd.3c00332 |
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2023 Other Outputs Electrochemical reactor and processes using the electrochemical reactorKappe, Oliver, Sommer, Florian and Cantillo, David (2023). Electrochemical reactor and processes using the electrochemical reactor. WO2023180283A2. |
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2023 Journal Article Scaling-up electroorganic synthesis using a spinning electrode electrochemical reactor in batch and flow modePetrović, Nikola, Malviya, Bhanwar K., Kappe, C. Oliver and Cantillo, David (2023). Scaling-up electroorganic synthesis using a spinning electrode electrochemical reactor in batch and flow mode. Organic Process Research and Development, 27 (11), 2072-2081. doi: 10.1021/acs.oprd.3c00255 |
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2023 Journal Article Metal‐free electrochemical reduction of disulfides in an undivided cell under mass transfer controlMalviya, Bhanwar K., Hansen, Eric C., Kong, Caleb J., Imbrogno, Joseph, Verghese, Jenson, Guinness, Steven M., Salazar, Chase A., Desrosiers, Jean‐Nicolas, Kappe, C. Oliver and Cantillo, David (2023). Metal‐free electrochemical reduction of disulfides in an undivided cell under mass transfer control. Chemistry: A European Journal, 29 (66) e202302664, 1-7. doi: 10.1002/chem.202302664 |
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2023 Journal Article Electrochemical nickel-catalyzed C(sp3)–C(sp3) cross-coupling of alkyl halides with alkyl tosylatesIbrahim, Malek Y. S., Cumming, Graham R., Gonzalez de Vega, Raquel, Garcia-Losada, Pablo, de Frutos, Oscar, Kappe, C. Oliver and Cantillo, David (2023). Electrochemical nickel-catalyzed C(sp3)–C(sp3) cross-coupling of alkyl halides with alkyl tosylates. Journal of the American Chemical Society, 145 (31), 17023-17028. doi: 10.1021/jacs.3c07313 |
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2023 Journal Article Control of a complex multistep process for the production of mesalazineCastillo, Ismael, Rehrl, Jakob, Sagmeister, Peter, Lebl, Rene, Kruisz, Julia, Celikovic, Selma, Sipek, Martin, Kirschneck, Dirk, Horn, Martin, Sacher, Stephan, Cantillo, David, Williams, Jason D., Khinast, Johannes G. and Kappe, Oliver (2023). Control of a complex multistep process for the production of mesalazine. Journal of Process Control, 122, 59-68. doi: 10.1016/j.jprocont.2022.12.009 |
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2022 Journal Article Panel discussion on... FLOW CHEMISTRYCantillo, David, Monedero, Martin, Dapremont, Olivier, Lusso, Carlo, McLaws, Mark, Blocher, Thomas, Wiles, Charlotte, Houldsworth, Stephen, Vizza, Alessandra, Hornung, Christian H., Kaaden, Anne, Stam, Wouter, McKay, Chris, Katz, Marianna, Borukhova, Svetlana, Kirschneck, Dirk, Ni, Xiong-Wei, Guillermin, Jean-Baptiste, Rouchet, Jean-Baptiste, Yazdanpanah, Nima, Roletto, Jacopo, Jenkins, Gareth, Poechlauer, Peter, Nuño, Manuel and Adamo, Andrea (2022). Panel discussion on... FLOW CHEMISTRY. Chimica Oggi, 40 (4), 16-41. |
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2022 Journal Article Sustainable synthesis of noroxymorphone via a key electrochemical N-demethylation stepSommer, Florian, Gerber Aeschbacher, Roman, Thurnheer, Urs, Kappe, C. Oliver and Cantillo, David (2022). Sustainable synthesis of noroxymorphone via a key electrochemical N-demethylation step. ACS Sustainable Chemistry and Engineering, 10 (27), 8988-8996. doi: 10.1021/acssuschemeng.2c02824 |
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2022 Journal Article Electrochemical oxidation of alcohols using nickel oxide hydroxide as heterogeneous electrocatalyst in batch and continuous flowJud, Wolfgang, Salazar, Chase A., Imbrogno, Joseph, Verghese, Jenson, Guinness, Steven M., Desrosiers, Jean-Nicolas, Kappe, C. Oliver and Cantillo, David (2022). Electrochemical oxidation of alcohols using nickel oxide hydroxide as heterogeneous electrocatalyst in batch and continuous flow. Organic Process Research and Development, 26 (5), 1486-1495. doi: 10.1021/acs.oprd.2c00064 |
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2022 Journal Article Synthesis of active pharmaceutical ingredients using electrochemical methods: keys to improve sustainabilityCantillo, David (2022). Synthesis of active pharmaceutical ingredients using electrochemical methods: keys to improve sustainability. Chemical Communications, 58 (5), 619-628. doi: 10.1039/d1cc06296d |
