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2021 Journal Article Continuous flow synthesis of a blocked polyisocyanate: process intensification, reaction monitoring via in-line FTIR analysis, and comparative life cycle assessmentGlotz, Gabriel, Waniek, Katharina, Schöggl, Josef-Peter, Cantillo, David, Stueckler, Clemens, Arzt, Anton, Gollner, Andreas, Schipfer, Rudolf, Baumgartner, Rupert J. and Kappe, C. Oliver (2021). Continuous flow synthesis of a blocked polyisocyanate: process intensification, reaction monitoring via in-line FTIR analysis, and comparative life cycle assessment. Organic Process Research and Development, 25 (10), 2367-2379. doi: 10.1021/acs.oprd.1c00329 |
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2021 Journal Article A small footprint oxycodone generator based on continuous flow technology and real-time analyticsSommer, Florian, Cantillo, David and Kappe, C. Oliver (2021). A small footprint oxycodone generator based on continuous flow technology and real-time analytics. Journal of Flow Chemistry, 11 (4), 707-715. doi: 10.1007/s41981-021-00193-y |
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2021 Journal Article Electrochemical α-arylation of ketones via anodic oxidation of in situ generated silyl enol ethersJud, Wolfgang, Sommer, Florian, Kappe, C. Oliver and Cantillo, David (2021). Electrochemical α-arylation of ketones via anodic oxidation of in situ generated silyl enol ethers. The Journal of Organic Chemistry, 86 (22), 16026-16034. doi: 10.1021/acs.joc.1c01224 |
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2021 Journal Article One-pot multistep electrochemical strategy for the modular synthesis of epoxides, glycols, and aldehydes from alkenesJud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2021). One-pot multistep electrochemical strategy for the modular synthesis of epoxides, glycols, and aldehydes from alkenes. Electrochemical Science Advances, 1 (3) e2100002, 1-9. doi: 10.1002/elsa.202100002 |
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2021 Journal Article Chemoselective electrochemical oxidation of secondary alcohols using a recyclable chloride-based mediatorCantillo, David, Sommer, Florian and Kappe, C. Oliver (2021). Chemoselective electrochemical oxidation of secondary alcohols using a recyclable chloride-based mediator. Synlett, 33 (02), 166-170. doi: 10.1055/a-1511-8869 |
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2021 Journal Article Advanced real-time process analytics for multistep synthesis in continuous flowSagmeister, Peter, Lebl, Rene, Castillo, Ismael, Rehrl, Jakob, Kruisz, Julia, Sipek, Martin, Horn, Martin, Sacher, Stephan, Cantillo, David, Williams, Jason D. and Kappe, C. Oliver (2021). Advanced real-time process analytics for multistep synthesis in continuous flow. Angewandte Chemie-International Edition, 60 (15), 8139-8148. doi: 10.1002/anie.202016007 |
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2021 Journal Article Flow technology for telescoped generation, lithiation and electrophilic (C3) functionalization of highly strained 1-azabicyclo[1.1.0]butanesMusci, Pantaleo, von Keutz, Timo, Belaj, Ferdinand, Degennaro, Leonardo, Cantillo, David, Kappe, C. Oliver and Luisi, Renzo (2021). Flow technology for telescoped generation, lithiation and electrophilic (C3) functionalization of highly strained 1-azabicyclo[1.1.0]butanes. Angewandte Chemie-International Edition, 60 (12), 6395-6399. doi: 10.1002/anie.202014881 |
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2021 Journal Article Electrochemically enabled one‐pot multistep synthesis of C19 androgen steroidsSommer, Florian, Kappe, C. Oliver and Cantillo, David (2021). Electrochemically enabled one‐pot multistep synthesis of C19 androgen steroids. Chemistry: A European Journal, 27 (19), 6044-6049. doi: 10.1002/chem.202100446 |
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2021 Journal Article Sustainable electrochemical decarboxylative acetoxylation of aminoacids in batch and continuous flowKöckinger, Manuel, Hanselmann, Paul, Roberge, Dominique M., Geotti-Bianchini, Piero, Kappe, C. Oliver and Cantillo, David (2021). Sustainable electrochemical decarboxylative acetoxylation of aminoacids in batch and continuous flow. Green Chemistry, 23 (6), 2382-2390. doi: 10.1039/d1gc00201e |
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2020 Journal Article A continuous flow bromodimethylsulfonium bromide generator: application to the synthesis of 2-arylaziridines from styrenesPrieschl, Michael, Cantillo, David and Kappe, C. Oliver (2020). A continuous flow bromodimethylsulfonium bromide generator: application to the synthesis of 2-arylaziridines from styrenes. Journal of Flow Chemistry, 11 (2), 117-125. doi: 10.1007/s41981-020-00125-2 |
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2020 Journal Article Continuous on demand generation of acrolein from glycerol using a reactive distillation strategyStrauss, Franz J., Pöchlauer, Peter, Schuster, Christian, Kohls, Paul, Steinhofer, Stefan, Zinganell, Christopher, Gutmann, Bernhard, Cantillo, David and Kappe, C. Oliver (2020). Continuous on demand generation of acrolein from glycerol using a reactive distillation strategy. Chimica Oggi/Chemistry Today, 38 (6), 24-27. |
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2020 Journal Article Development and assembly of a flow cell for single‐pass continuous electroorganic synthesis using laser‐cut componentsJud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2020). Development and assembly of a flow cell for single‐pass continuous electroorganic synthesis using laser‐cut components. Chemistry–Methods, 1 (1), 36-41. doi: 10.1002/cmtd.202000042 |
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2020 Journal Article Organomagnesium based flash chemistry: continuous flow generation and utilization of halomethylmagnesium intermediatesvon Keutz, Timo, Cantillo, David and Kappe, C. Oliver (2020). Organomagnesium based flash chemistry: continuous flow generation and utilization of halomethylmagnesium intermediates. Organic Letters, 22 (19), 7537-7541. doi: 10.1021/acs.orglett.0c02725 |
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2020 Journal Article Electrochemical N-demethylation of 14-hydroxy morphinans: sustainable access to opioid antagonistsGlotz, Gabriel, Kappe, C. Oliver and Cantillo, David (2020). Electrochemical N-demethylation of 14-hydroxy morphinans: sustainable access to opioid antagonists. Organic Letters, 22 (17), 6891-6896. doi: 10.1021/acs.orglett.0c02424 |
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2020 Journal Article A continuous flow cell for high‐temperature/high‐pressure electroorganic synthesisJud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2020). A continuous flow cell for high‐temperature/high‐pressure electroorganic synthesis. ChemElectroChem, 7 (13), 2777-2783. doi: 10.1002/celc.202000696 |
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2020 Journal Article Organophotocatalytic N‐demethylation of oxycodone using molecular oxygenChen, Yuesu, Glotz, Gabriel, Cantillo, David and Kappe, C. Oliver (2020). Organophotocatalytic N‐demethylation of oxycodone using molecular oxygen. Chemistry: A European Journal, 26 (13), 2973-2979. doi: 10.1002/chem.201905505 |
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2020 Journal Article Translating batch electrochemistry to single-pass continuous flow conditions: an organic chemist’s guideMaljuric, Snjezana, Jud, Wolfgang, Kappe, C. Oliver and Cantillo, David (2020). Translating batch electrochemistry to single-pass continuous flow conditions: an organic chemist’s guide. Journal of Flow Chemistry, 10 (1), 181-190. doi: 10.1007/s41981-019-00050-z |
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2019 Journal Article Continuous flow synthesis of terminal epoxides from ketones using in situ generated bromomethyl lithiumvon Keutz, Timo, Cantillo, David and Kappe, C. Oliver (2019). Continuous flow synthesis of terminal epoxides from ketones using in situ generated bromomethyl lithium. Organic Letters, 21 (24), 10094-10098. doi: 10.1021/acs.orglett.9b04072 |
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2019 Journal Article Continuous flow synthesis of methyl oximino acetoacetate: accessing greener purification methods with inline liquid–liquid extraction and membrane separation technologyLebl, René, Murray, Trevor, Adamo, Andrea, Cantillo, David and Kappe, C. Oliver (2019). Continuous flow synthesis of methyl oximino acetoacetate: accessing greener purification methods with inline liquid–liquid extraction and membrane separation technology. ACS Sustainable Chemistry and Engineering, 7 (24), 20088-20096. doi: 10.1021/acssuschemeng.9b05954 |
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2019 Journal Article Cathodic C–H trifluoromethylation of arenes and heteroarenes enabled by an in situ-generated triflyltriethylammonium complexJud, Wolfgang, Maljuric, Snjezana, Kappe, C. Oliver and Cantillo, David (2019). Cathodic C–H trifluoromethylation of arenes and heteroarenes enabled by an in situ-generated triflyltriethylammonium complex. Organic Letters, 21 (19), 7970-7975. doi: 10.1021/acs.orglett.9b02948 |
